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有机化学实验【2025|PDF下载-Epub版本|mobi电子书|kindle百度云盘下载】

陈秋云主编；曲玲玲，陆晓青，范伟强，闫早学副主编著
出版社：镇江：江苏大学出版社
ISBN：9787568401920
出版时间：2016
标注页数：119页
文件大小：9MB
文件页数：125页
主题词：有机化学－化学实验－高等学校－教材－英文

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图书目录

Part 1 Basic Knowledge in Organic Chemistry Laboratory1

1.1 Rules in laboratory1

1.2 Prevention and treatment of the common accidents in laboratory1

1.3 Requirements of preparation，record and report of experiments7

1.4 Common lab equipment and apparatus8

1.5 Waste disposal10

Part 2 Basic Experimental Techniques12

2.1 Preparation of organic compounds12

2.2 The determination of physical constants of organic compounds16

2.3 Separation and purification technology of organic compounds25

2.4 Spectral analysis technology of organic compounds46

Part 3 Experiments for Preparation of Organic Compounds57

3.1 Preparation of cyclohexene57

3.2 Preparation of anhydrous ethanol59

3.3 Preparation of n-butyl bromide61

3.4 Preparation of n-butyl ether63

3.5 Preparation of acetophenone66

3.6 Preparation of aspirin68

3.7 Preparation of cinnamic acid71

3.8 Preparation of n-butyl acetate73

3.9 Preparation of isoamyl acetate76

3.10 Synthesis of glycerol monostearate78

3.11 Preparation of skin care cosmetic81

3.12 Preparation of detergent84

Part 4 Extraction，Separation and Identification of Organic Compounds88

4.1 Distilling 95％ethanol and measuring the boiling point88

4.2 Recrystallization of benzoic acid89

4.3 Purification of benzaldehyde90

4.4 Isolation of cafieine from tea leaves92

4.5 The extraction of limonene from orange peels94

4.6 Separation of A and B by thin-layer chromatography96

4.7 Separation of spinach pigments by column chromatography97

4.8 Preparation and resolution for optical isomers of tris（ethylenediamine）cobalt salts101

4.9 Identification of sugar105

4.10 Identification of amino acids and proteins107

Reference110

Appendix：Experimental Graphs and Properties of Organic Solvents111

Ⅰ．Distilling 95％ethanol and measuring the boiling point111

Ⅱ．Recrystallization of benzoic acid113

Ⅲ．Isolation of caffeine from tea leaves and sublimation116

Ⅳ．Synthesis，isolation and purification of n-butyl acetate117

Ⅴ．Physical constant119